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Combined data mining strategy for the systematic identification of sport drug metabolites in urine by liquid chromatography time-of-flight mass spectrometry.

Domínguez-Romero JC, García-Reyes JF, Martínez-Romero R, Berton P, Martínez-Lara E, Del Moral-Leal ML, Molina-Díaz A.SourceAnalytical Chemistry Research Group, Department of Physical and Analytical Chemistry, University of Jaén, 23071 Jaén, Spain.
Analytica chimica acta.Anal Chim Acta.2013 Jan 25;761:1-10. doi: 10.1016/j.aca.2012.11.049. Epub 2012 Dec 5.
The development of comprehensive methods able to tackle with the systematic identification of drug metabolites in an automated fashion is of great interest. In this article, a strategy based on the combined use of two complementary data mining tools is proposed for the screening and systematic detec
PMID 23312308

Efficacy and safety of modified sequential three-step empirical therapy for chronic cough.

Wei W, Yu L, Wang Y, Li X, Qiu Z, Wang L, Liu B, Liang S, Lü H, Qiu Z.SourceDepartment of Respiratory Medicine, Tongji Hospital, Tongji University School of Medicine, Shanghai, China.
Respirology (Carlton, Vic.).Respirology.2010 Jul;15(5):830-6. doi: 10.1111/j.1440-1843.2010.01785.x. Epub 2010 Jun 9.
BACKGROUND AND OBJECTIVE: Sequential three-step empirical therapy is useful for the management of chronic cough. The purpose of this study was to evaluate the efficacy and safety of modified sequential three-step empirical therapy.METHODS: Consecutive patients (n = 240) with chronic cough were recru
PMID 20546197

関根均,中原雄二
衛生化学 37(6), 537-541, 1991-12-31
… solution of 0.5% BNQ-sulfonate, 200μl of methoxyphenamine (1μg/ml) as an internal standard and 100μl of methanol, as a shift agent of interference peak was warmed at 40℃ for 20 min. The reaction solution was extracted with n-hexane-ether (1 : 1) and the solvent was evaporated under N_2. … dose of MA hydrochloride at 7.3,7.8,10.2,20.4,31 and 66.5h earlier were analysed to confirm the use of MA. …
NAID 110003641767

世一義隆 [他],佐野彰,上野政一
分析化学 20(1), 104-106, 1971
… color reaction of secondary amine with carbon disulfide and copper(II) has been applied to the colonmetric determination of methoxyphenamine hydrochloride in mixed pharmaceutical preparations.<BR>Methoxyphenamine hydrochloride was treated with carbon disulfide in an ammoniacal solution to form dithiocarbamic acid which reacted with copper(II) to form a yellow complex.<BR>The absorbance measured at 438 mμ against the reagent blank obeyed Beer's law in the …
NAID 130000942248